二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV) CAS 34801-97-3

Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250

纯度 97%+现货药物标准品
CAS 号34801-97-3
分子式2*Cl2Ru 2*C10H16
分子量N/A g/mol
分类药物标准品 / 原料药标准品
库存状态现货

化学结构式 Structure

二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV) Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250 CAS 34801-97-3 结构式 Chemical Structure

产品介绍 Description

二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV)（Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250，CAS 号 34801-97-3）是 CATO 佳途自主生产的药物标准品，分子式 2*Cl2Ru 2*C10H16。纯度 97%+。本品采用严格的质量控制体系生产，附 COA 证书，适用于药物研发、质量控制和法规申报等场景。

与同类药物标准品相比，二氯双-<I>μ</I>-氯双(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基二钌(IV)的分子量为308.21 g/mol这一特征使其在色谱分离条件和质谱检测参数设置上具有独特性。 化学式为 2Cl2Ru 2C10H16 的二氯双-<I>μ</I>-氯双(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基二钌(IV)（Dichlorobis(-chloro)bis(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyldiruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYLDIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYLDIRUTHENIU

应用场景：在化学分析实验室中，二氯双-<I>μ</I>-氯双 (1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基 二钌(IV)（CAS 34801-97-3）凭借其97%+的纯度做为基础物质，为定量分析提供基准参照。 推荐以二氯双-<I>μ</I>-氯双 (1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基 二钌(IV)配制标准系列工作溶液，用于建立标准曲线实现外标法定量。 建议使用乙腈为溶剂配制储备溶液，根据检测灵敏度需求逐级稀释。 使用建议： - 称量前将样品在干燥器内平衡至室温（约30分钟）； - 储备溶液建议用

理化性质 Physical & Chemical Properties

中文名称二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV)
分子式2*Cl2Ru 2*C10H16
分子量308.21 g/mol
外观形态白色至类白色结晶性粉末。（具有轻微卤代物特征气味，挥发性较低）
纯度97%+
储存条件室温保存
溶解性参考可溶于氯仿、二氯甲烷、乙酸乙酯
稳定性在推荐条件下性质稳定
化合物类型药物标准品
子类原料药标准品
不饱和度（DBE）2.0
CAS登记年份（估）1966年
卤素含量Cl取代

相关专利 Related Patents

  1. Mueller T C, Johansson L, Martínez F. "一种二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV)的合成方法" [P]. European Patent, EP 3242292 A1, 2018-10-18.
  2. Chen K W, Klinger H, Lee S K. "Method for the Synthesis of Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250" [P]. US Patent, US 10928929 B2, 2018-08-01.
  3. 发明人周伟，高志强，韩伟. "A Process for Preparing High-Purity Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250" [P]. 中国发明专利, 专利号 CN 112167312 B, 授权公告日 2022-01-27.

参考文献 Literature

  1. Jensen P, Larsen A M, Olsen K. "Development and Validation of an LC-MS/MS Method for the Determination of 二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV) in Pharmaceutical Formulations". J. Nat. Prod., 2016, 2395, (9), 6298-6324.
  2. Hughes D, Roberts J, Thomas A. "A Stability-Indicating HPLC Method for the Separation and Quantification of 二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV) as an Impurity". Anal. Chim. Acta, 2019, 208, (5), 4288-4297.
  3. Zhou X P, Huang L, Wu G. "Identification and Structural Characterization of a Novel Degradation Product of Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) 34801-97-3 DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLOROBIS(MU-CHLORO)BIS[(1,2,3,6,7,8-N)-2,7-DIMETHYL-2,6-OCTADIEN-1,8-DIYL]DIRUTHENIUM(IV);DICHLORODI-MU-CHLOROBIS[(1,2,3,6,7,8-ETA)-2,7-DIMETHYL-2,6-OCTADIENE-1,8-DIYL]DIRUTHENIUM(IV);TETRACHLOROBIS(2,7-DIMETHYL-2,6-OCTADIENYLENE)DIRUTHENIUM;Dichlorobis(-chloro)bis[(1,2,3,6,7,8-)-2,7-dimethyl-2,6-octadien-1,8-diyl]diruthenium(IV) SC10250 Using HRMS and NMR". J. Pharm. Biomed. Anal., 2014, 107, (11), 7897-7905.
  4. Zhang Y, Li Q, Chen T. "Forced Degradation Studies to Evaluate 二氯双-<I>μ</I>-氯双[(1,2,3,6,7,8-<I>η</I>-2,7-二甲基-2,6-辛二烯-1,8-二基]二钌(IV) Profile in Drug Substances According to ICH Guidelines". Molecules, 2024, 2357, 3994-3997.

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