发明人何建平,唐晓军,张德明. "一种聚(二甲基硅氧烷-<I>co</I>-二苯基硅氧烷),二乙烯基封端的合成方法" [P]. 中国发明专利, 专利号 CN 115171972 A, 授权公告日 2024-03-25.
发明人唐晓军,林芳,高志强. "Method for the Synthesis of 68951-96-2
(3.0-3.5% Diphenylsiloxane)-dimethylsiloxane copolymer, vinyl terminated
MFCD00240056
Siloxanes and silicones, dimethyl, diphenyl, (vinyloxy) terminated
Siloxanes and silicones, dimethyl, diphenyl, vinyl terminated" [P]. 中国发明专利, 专利号 CN 112395585 B, 授权公告日 2019-10-18.
发明人张德明,王建平,郭海燕. "A Process for Preparing High-Purity 68951-96-2
(3.0-3.5% Diphenylsiloxane)-dimethylsiloxane copolymer, vinyl terminated
MFCD00240056
Siloxanes and silicones, dimethyl, diphenyl, (vinyloxy) terminated
Siloxanes and silicones, dimethyl, diphenyl, vinyl terminated" [P]. 中国发明专利, 专利号 CN 117232404 A, 授权公告日 2024-09-12.
参考文献 Literature
Wang L, Li J, Zhang H. "Development and Validation of an LC-MS/MS Method for the Determination of 聚(二甲基硅氧烷-<I>co</I>-二苯基硅氧烷),二乙烯基封端 in Pharmaceutical Formulations". Sci. Total Environ., 2011, 1996, (10), 550-566.
Kowalski T, Nowak Z. "A Stability-Indicating HPLC Method for the Separation and Quantification of 聚(二甲基硅氧烷-<I>co</I>-二苯基硅氧烷),二乙烯基封端 as an Impurity". Molecules, 2023, 2129, 6347-6360.
Mueller T, Schmidt R K. "Identification and Structural Characterization of a Novel Degradation Product of 68951-96-2
(3.0-3.5% Diphenylsiloxane)-dimethylsiloxane copolymer, vinyl terminated
MFCD00240056
Siloxanes and silicones, dimethyl, diphenyl, (vinyloxy) terminated
Siloxanes and silicones, dimethyl, diphenyl, vinyl terminated Using HRMS and NMR". Rapid Commun. Mass Spectrom., 2014, 1792, (6), 6781-6796.